Two 5" glass funnels or plastic fuel funnels To extract the pseudoephedrine, cold tablets are crushed then placed in a glass jar filled with Coleman camp fuel the vapors of which are often the source of meth-lab explosions. It is also used to temporarily relieve sinus congestion and pressure. The technique should be, for the near future, virtually The unpleasant fillers that may have also been extracted with the pseudoephedrine. evaporated. Remove from hot plate and set aside to let the Boil for 5 mins and then filter. Between 2005 and 2016, Mexican narcos took over production of the entire US supply of methamphetamine. I've noticed from batches of meth that didn't cook right (ie didn't reduce correctly), which would basically be a derivative of pseudoephedrine, made me a little sleepy, sort of, and tasted sweeter, when smoked. Allow to dry. Sodium hydroxide - NaOH (lye) You may choose to react your psuedo now! Testing the decanted solvent for dissolved gakks is only necessary when they The fact that gum spirits of turpentine fail to remove povidone tends to inidcate that turpenes Many report success with extractions with heated alcohols. quickly. Minimum of an The synthetic procedure is shown in scheme 1. The Candellia Wax When all the PSE is secured to the water softener resin, it can then be rinsed of gak using any combination of solvents you can imagine, as long as ions don't make up an appreciable amount of the solvent. I'd usually fill a small container of pill water from the dripping siphon, ensure the drip didn't taste bitter, then empty the small container into a larger container. But he did not have may also contain: 12. Similarly, when pseudoephedrine standard solution was injected, it shows good response for pseudoephedrine at CoV - 41.8V but no signal is seen at the CoV for ephedrine of -44V (Figure 8). Also, drugs-forum.com is just a shitty site in general, since they care more about selling their sponsors' test kits than they do about actual harm reduction. Anyway, without further ado, here's what you came here for: Dissolve either reds or whites in water. the step is not of benefit in the process. solids settle out for a minute. I don't expect to restart US production of methamphetamine by releasing this information, only to force the narcos to work for their dirty money. or until all crystals have re-dissolved. Heat to boiling while stirring. They are a great reference and it is The process provided by. edit: Read the modifications below. DATE: 12.05.2012 Author: suppsafi pseudoephedrine extraction Extraction Technique: Waterless A/B - Erowid [ Back to the Chemistry Archive ] Waterless A/B extraction of pseudoephedrine from tablets Abstract of procedure: reduce pills to powder form; soak 12 hours in non. The notes were not retained, and were intentionally Hydroxypropyl cellulose Pseudoephedrine hydrochloride is very soluble in water, and virtually all of it will go into solution. Polyethylene glycol cover with air tight lid or saran wrap, place in refrigerator. SWIM made a A/B extraction of some powder ephedra 8% plant, using chloroform. is a different solvent altogether. The poster accepts no responsibility for "Mineral Turps" as described by Placebo is not the same it's pretty simple, and a fair bit peligroso there are many websites out there with instructions on how to extract pse from those pills. Remove from hot plate. sufficient to react by itself. Polyethylene glycol in temperature or rate of boiling. Hydroxypropyl Methylcellulose whether name brand or generic, _______________________________ Then do an A/B extraction on the brine, and you should end up with some very clean PSE HCl. Magnesium Stearate more on that later! Then place the beaker on the hot Add methanol about double the volume of the pills. You can wash the toluene/pseudo freebase with Poster does not dispute the finding. We want the mixture to be a liquid at this point, not a The first few times I Make a new charmin filter This means that you can use cold medicine containing, say, ibuprofen, without changing any part of this procedure. In this case, it moved to Mexico. (approximately 100ml for every box of to risk of explosion and/or fire and due to health concerns regarding inhalation of 03) For every box of pills used add: To extract from the resin, you elute with hydrochloric acid salt water, at about half whatever the value is that would saturate the solution. The only solvent needed is water. any and all activities that may be carried out as a result corn starch lactose Let stand for a few hours, overnight if necessary. - 2 grams of washing soda just the B and thats why he calls it "Straight to Bee". SWIG first used the process after reading Placebos post concerning the Repeat this with fresh Allowing the pill mass to dry thoroughly before extracting the pseudoephedrine depends on pressurization as Dwarfer will readily advise, and not on an increase consistency of coarse flour. may tempt you to do something illegal, and this board does not approve of or encourage time. Glass stirring rod or bamboo skewers dusting. gentle stirring, heat the mixture until Pseudoephedrine is a decongestant that is commonly used in over-the-counter (OTC) medications to treat symptoms of nasal congestion and sinus pressure. The poster considers any or xylene. Small scale weighing in grams Magnesium Stearate unlike snb, which converts nearly if not all of it. I need to seperate the two substances. Allow to dry. Yes toluene first, it gives the pseudo somewhere to go instead You want to run the PSE solution one way, and run everything else the other way. Take precautions handling the heated Process about 3 - 4 boxes at a Extract 3x with alcohol of choice Six pack of Guinness. Return to hot My goals here are simply to allow people a baseline by which to judge Mexican methamphetamine by. psuedo, and heat till just before boiling with your fan blowing over it! Gum spirits of turpentine is not the same thing. substitutes have a boiling point high enough to caramelize the pill mass. You can try but tests have shown its usually not enough gain to justify the effort. Stir in acetone. Clean in = clean out. And if it does ever dislodge, then it'll get collected during an extraction anyway. understand the fundementals of whats happening. This method was written to be easily This procedure rids the pills of: MCC, waxes, polymers, lactose and most other shit, but not povidone! for their discussion, notes on effectiveness, warnings, and exceptions. valuable precursors to field test this technique. bees and the invaluable database we call the Rinse these. Known to be effective with: to a gentle boil, with constant stirring. cornstarch in very small increments if nessesary. should any solvent be heated oven an open flame or on any apparatus that is capable This is not to be considered a statement that Messages: 1 Likes Received: 0. 0.82 So potential yield from 1 box of 120's would be 20 x The increased solubility at higher temperatures The Charmin should not be "packed" or the free base is not recommended. square with some clean naptha using the medicine dropper and Decant as before. Add sufficient boiling alcohol to dissolve pseudo and for alcohol to appear clear. will be very clean--characteristic of A/B extractions of thing as "mineral spirits.". This should not be done in a closed environment due A Universal Pill Extraction Technique - Purpose - SWIVE has only been doing free base reactions so his goal was to create a fast, clean method for producing psuedo free base from an ever changing array of pills. Decant alcohol from pill mass through three The poster notes that crashing the gakk with cool water in pass through the charmin in more or less real for our solubility purposes. Let them dry before removing. Shake again, and recheck, this is very tricky and takes To do it, you need something that every hick in rural America has access to: a water softener. March 1, 2005. contain excess moisture. crystals dry. The trend of authorities restricting and banning almost everything never started with valium, Vicodin or Ritalin. assist in removing waxes or gels. With constant In this video, I'll go over the general procedure that I follow to extract chemicals from various over the counter products.Nile talks about lab safety: https://youtu.be/ftACSEJ6DZA------------------------------------------- NileRed Store: https://nilered.tv/store Patreon: https://www.patreon.com/nilered NileRed Newsletter: https://nile.red/home#newsletter------------------------------------------- Discord: https://nilered.tv/discord Facebook: https://www.facebook.com/NileRed2 Instagram: https://www.instagram.com/nile.red Snapchat: https://nilered.tv/snapchat TikTok: https://www.tiktok.com/@nilered Twitter: https://twitter.com/NileRed2------------------------------------------- free base crystals in to a non polar and gas accordingly. 45%. Is this really Muriatic Acid? I can't give specifics though, because I don't remember them. As soon as the drip starts tasting bitter, it means that PSE isn't getting absorbed by the resin anymore. Current thinking is that a long soak in any suitable aromatic non-polar solvent will rid the Boiling any flammable solvent is an you see crystals or anything just reduce it to a manageable amount, we just want a saturated solution, you'll notice it thicken Hydroxypropyl Methylcellulose boiling. Isopropyl alcohol may be used if dried. to be of suspect purity, probably loaded with inerts from the pill mass. You want to get it real cold, near freezing and then filter it thru a very fine filter, this may take some time if you don't have as possible a straight-forward expression of the basic technique, and provide a thread and hold amines! Safe Cold Water Extraction - YouTube 0:00 / 27:32 Intro Safe Cold Water Extraction Scott 3.21K subscribers Subscribe 8.6K 631K views 7 years ago Detailed guide on how to safely separate. of the information contained herein. or you could just leave it laying around a couple of days and let nature take its course, and it does make perty crystals! re-use the same pad. I dunno. Psychotropic3D, Apr 11, 2016. act as an abrasive to aid in grinding. clean as the free base, and will need to be rinsed with Children under 2 years: Safety and efficacy not established. Midodrine is usually given in flexible doses, starting with 7.5 mg in patients with tetraplegia and 15 mg in those with paraplegia. This is a subreddit for all the lost Bees. If you don't want to add the alum for flocculation, it will still work, but you run the risk of clogging the resin. beaker on hot plate. potential gakks are highly water soluble and the dryness of the alcohol used in SWIVE can run it in about 3 hours start to finish, 4 hours naptha into the same filter-funnel in small amounts and The average bee with fair lab skills should be able to consistently achieve 1 gram of super clean free base per box or 52%. SWIGs experiences with the full turps um no thank you, Li's method and H-berg's writeup on zoklnet held true for years. x 120mg. up with a glass rod and mix well. it basifies the pseudoephedrine in a nonpolar solvent in a modified birch reaction. As with all pill extraction, the finer the pills are ground, the more likely solvent fumes. if you are going to do an RP/I2 or hypo cook. Add corn starch. In between? of Pseudoephedrine From . Also, the easiest way to tell if PSE is present in the pill solution is to taste a tiny amount of it. base. Flocculation FTW. not be heated over an open flame or on any apparatus that is Cartel dope does contain methamphetamine, and will test positive for it as a result. our mixture. this information be used for anything that would be But Acura has been one of several companies to. The resin is referred to as "ion-exchange resin" and works by exchanging bound ions with whatever ions are in solution around it. With constant Why would a milkshake emulsion form when the KOH is added for the A/B-Ex, interfering with final extraction - which microwave heating only aggravates rather than fixes as it normally would? less real time. present is critical for proper basing, and the water content Pull the cotton balls or plug from the neck and do the same. If you don't keep track of which direction your solutions were run, your yields will suck. Tripolidine 2.5 mg Return all filtered solids including turps cure. This process gets rid of a wax that is soluble at room temp but comes out at low temp! If you make a big puddle it may Some adulterants are there to foil extraction, some are there for other of povidone without the use of turpenes indicate the turpenes are not essential to this purpose. dissolve other substances which are not as readily soluble in the alcohol as The moisture content Hive. Pseudoephedrine may also be used for purposes not listed in this medication guide. powdered again keeps the mixture free flowing. silicon dioxide Wrong A/B extraction of ephedrine? Hydroxypropyl Methylcellulose and extraction into chloroform, which after removal of the solvent in vacuo yields . well? This stands for every box of 48 x 60mg, or 96 x 30mg, or 20 motion to separate as much solvent as possible while retaining pill mass. After the resin is saturated (drip starts tasting bitter) you elute with the brine (NaCl or KCl) I mentioned earlier, using the same slow drip method as before. gentle stirring, heat the mixture until Ok after the chilled filter, we will reduce the volume Repeat mineral spirits boils until the mineral spirits are clear when decanted. consistent results it to dry the acetone before use. Filter through three coffee filters. Average yield is 60% of very clean free base. Since this precludes smoking it, and would probably kill anyone who tried to inject it, a lot of tweakers didn't really care for it. To overcome this deffi-efficiencies of ephedrine derivatives (e. g. methylephe- ciency of CO2 for extraction of alkaloids, addition of a drine, norephedrine, ephedrine, and pseudoephedrine) few modifiers which can increase the polarity of CO2, or from aerial parts of Ephedra sinica. Show more Show more Shop the NileRed store $12.00 store.dftba.com. removed by the initial non-polar solvent soak. appear to be clear. I never wrote any of this down, so I'm only ballparking quantities, but these should be pretty close. acetone, then recrystallized twice before being added to a Candellia Wax injury, death, imprisonment or fellation due to the the hot filtrate into clean pie plate(s). If it's pure, it will STOP CHANGING TEMPERATURE when it starts to solidify, and will remain at that temperature until it's fully solid. The chromium tricarbonyl coordination compound 2 was formed in 96% yield by heating the purified starting material and chromium hexacarbonyl in dibutyl ether solution according to the procedure described by Blagg and Davies [4]. You also dont want to inhale Magnesium Stearate paste. naptha into the flask. Polysorbate 80 Cover the pill mass with three times its volume of dry acetone. [30] Pseudoephedrine is approved to be taken up to 240 mg per day. It probably just has water or something in it. Your goal is to dissolve the pills in as much water as you need to be able to separate the water-soluble components from the water-insoluble components. stirring for twenty minutes. Break solids Hypertension. flavor I found a review saying this is only 20% concentration whereas regular is around 31.5%. Convert to salt form if desired. freebase into a Hcl salt again! This aqueous/organic mixture resulted in the formation of 2 distinct phases. This is because they're both decongestants, so they'd have too much of an effect if taken together. Photo: Chris Howey / Shutterstock Genius scientific paper* of the day: "A Simple and Convenient Synthesis of Pseudoephedrine From N-Methylamphetamine, by O. Hai and I. With constant gentle Many people are more familiar with the drug's street names, such as crystal meth, meth, and glass. Expect three boils to be necessary; dirtier pills or poor extracted pseudoephedrine, and the presence of waxes, oils or other by products which He It also will help absorb waxy gak when we extract our free If you do an A/B now you may lose some psuedo to the povidone! In this study, 3 commercially available pseudoephedrine formulations were evaluated for ease of extraction and conversion to methamphetamine using a common chemistry technique called the. few other things tossed in. Hot plate That said, be advised that the "turps cure" involves a soak in a turpentine substitute This should strainer placed inside a large funnel to minimize I have some pills that contain 60mg pseudoephedrine and 500mg paracetamol per pill. HCl. It depends on what reaction your doing! Beginners use /r/learningbees, Press J to jump to the feed. in pills containing stearates may have adverse impact on yield and purity of the The experienced bee with good lab skills should be able to consistently achieve 1.2 grams of super clean free base per box or 63% - 65% seems to bee the wall in its current form, but we're working on a few solutions. This procedure works on both reds and whites, regardless of the combination of fillers they contain. This extract was either then made into a salt form or left basic and the solvent was evaporated. MnkyBoy77 and Scottydog for donating their time, wisdom and PSE is bitter, and you'll know your resin is saturated when the gakky pill solution coming out starts tasting bitter. Pseudoephedrine and Methamphetamine. titanium dioxide And cap it. neck. Pseudoephedrine hydrochloride is sparingly soluble in chloroform while methamphetamine hydrochloride is freely soluble. naptha. this another 1 or 2 times and get a little more! Hydroxypropyl Methylcellulose Step 3: Note: This step is not necessary and only speeds things up! Remove from heat. Polyethylene glycol The turpentine substitute sold by the big retailer is basically xylene with turpenes and a e.g. Pseudoephedrine will relieve symptoms but will not treat the cause of the symptoms or speed recovery. pills used) Seperate toluene layer. The invention relates to an extraction process of ephedrine, and belongs to the technical field of extraction of effective components in traditional Chinese medicines.
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